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X-ray Diffractometer (XRD)

X射线衍射仪(X-ray diffractometer,简称XRD)是目前研究晶体结构最有力的方法之一。XRD特别适用于晶态物质的物相分析,通过检查样品的X射线衍射图以及与已知的晶态物质的X射线衍射图谱的对比,可完成对样品物相组成和结构的定性鉴定。通过对样品衍射强度等数据的分析计算,可以完成样品物相组成的定量分析。

XRD还可测定材料中晶粒的大小及排布取向、材料中的应力测量、摇摆曲线、倒易空间图、结晶度、晶胞参数的精确测定等。

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Technical Specifications
Item Specifications
Dimensions 1300 (W) × 1880 (H) × 1300 (D) mm
X-ray tube Power: 2.2 kW, voltage: 10–60 kV, current: 0–50 mA
Target: Cu, anode grounded, Beryllium Window: 300 μm
Electron beam focal spot: 0.4 × 1.2 mm
Water cooling: Minimum flow rate: 3.5 l/min, maximum water pressure: 490 kPa, pressure drop: 98 kPa
High-voltage power supply Input: voltage 230 Vac – 10%, one phase, current 33 A
Output: voltage 0-60 kV, current 0-80 mA
Stability: < 0.01% voltage and current variation within 8 hours after a 1-hour warm-up period
Ripple: 0.03% rms below 1 kHz; 0.75% above 1 kHz rms
Goniometer Type: Vertically positioned goniometer
Angle range: -110°~ +168°
Angle positioning: Stepper motor + optical encoder
Minimum step size: 0.0001°, positioning accuracy: < 0.0005°

 

Item Specifications
Detector Type: Photon counter detector (2D)
Active area: 77.1×38.4 = 2961 mm2
Pixel size: 75×75 μm
Size: 100×140×93 mm3
Sample stage Standard sample stage: Rx, Ry, Z, Phi
XYZ motion stage (optional): X, Y, Z
Capillary sample stage (optional): X, Y, Phi
Five-axis sample stage (optional): X, Y, Z, Phi, Chi
Non-ambient sample stage (optional)
Optical elements Variable slit: 0.05 – 10 mm
Soller Slits: 0.5°, 0.2°, 0.1°, 0.05°, 0.02°
Goebel mirror: Divergence 0.03°, f1 = 100 mm, monochromaticity Kα
Double crystal monochromator: Ge220×2

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