X射线衍射仪(X-ray diffractometer,简称XRD)是目前研究晶体结构最有力的方法之一。XRD特别适用于晶态物质的物相分析,通过检查样品的X射线衍射图以及与已知的晶态物质的X射线衍射图谱的对比,可完成对样品物相组成和结构的定性鉴定。通过对样品衍射强度等数据的分析计算,可以完成样品物相组成的定量分析。
XRD还可测定材料中晶粒的大小及排布取向、材料中的应力测量、摇摆曲线、倒易空间图、结晶度、晶胞参数的精确测定等。
Item | Specifications |
---|---|
Dimensions | 1300 (W) × 1880 (H) × 1300 (D) mm |
X-ray tube | Power: 2.2 kW, voltage: 10–60 kV, current: 0–50 mA |
Target: Cu, anode grounded, Beryllium Window: 300 μm | |
Electron beam focal spot: 0.4 × 1.2 mm | |
Water cooling: Minimum flow rate: 3.5 l/min, maximum water pressure: 490 kPa, pressure drop: 98 kPa | |
High-voltage power supply | Input: voltage 230 Vac – 10%, one phase, current 33 A |
Output: voltage 0-60 kV, current 0-80 mA | |
Stability: < 0.01% voltage and current variation within 8 hours after a 1-hour warm-up period | |
Ripple: 0.03% rms below 1 kHz; 0.75% above 1 kHz rms | |
Goniometer | Type: Vertically positioned goniometer |
Angle range: -110°~ +168° | |
Angle positioning: Stepper motor + optical encoder | |
Minimum step size: 0.0001°, positioning accuracy: < 0.0005° |
Item | Specifications |
---|---|
Detector | Type: Photon counter detector (2D) |
Active area: 77.1×38.4 = 2961 mm2 | |
Pixel size: 75×75 μm | |
Size: 100×140×93 mm3 | |
Sample stage | Standard sample stage: Rx, Ry, Z, Phi |
XYZ motion stage (optional): X, Y, Z | |
Capillary sample stage (optional): X, Y, Phi | |
Five-axis sample stage (optional): X, Y, Z, Phi, Chi | |
Non-ambient sample stage (optional) | |
Optical elements | Variable slit: 0.05 – 10 mm |
Soller Slits: 0.5°, 0.2°, 0.1°, 0.05°, 0.02° | |
Goebel mirror: Divergence 0.03°, f1 = 100 mm, monochromaticity Kα | |
Double crystal monochromator: Ge220×2 |
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